Study on preparation process and properties of high purity indigestible dextrin
-
摘要: 研究了高纯度难消化糊精的制备工艺及其特性。以玉米淀粉为原料,经过高温酸解得到焦糊精,再酶解、浓缩,采用酒精沉淀的方法得到难消化糊精后用酒精洗去葡萄糖,制备高纯度难消化糊精。结果表明最佳工艺条件为:加酸量为12%,焦糊化温度为180℃,焦糊化时间为0.5h,酒精洗涤次数为6次,此时高纯度难消化糊精得率可达40.32%,纯度可达95.30%。并测定了高纯度难消化糊精的分子量分布和热特性分析,重均分子量为8607u,热稳定性高。本文为其在各类食品中的应用奠定了一定基础。Abstract: It was described the preparation and properties of high purity indigestible dextrin. The corn starch was acidhydrolyzed under 180℃ for 0.5h by adding 12% (V/W) HCl solution (1% W/W) firstly, and then mixed with 10 folds water (V/W) and enzymolyzed by amylase and glucoamylase. The hydrolysis was concentrated under vacuum and then precipitated with ethanol to be purified, the precipitation for 6 times was the production of indigestible dextrin and the yield was 40.32% and the purity was 95.30%. Analysis of molecular weight distribution and DSC-thermogram of high purity indigestible dextrin were studied, the results showed the high thermal stability and the heavy molecular weight was 8607 u, which provided some information for its application in all kinds of food.
-
Keywords:
- indigestible dextrin /
- high purity /
- preparation process /
- properties
-
[1] 寇秀颖, 黄冬冬, 王三永, 等.难消化糊精及其制备工艺[J].食品科技, 2007, 32 (9) :50-52. [2] Brouns F, Arrigoni E, Langkilde A M.Physiological and Metabolic Properties of a Digestion-Resistant Maltodextrin, Classified as Type 3 Retrograded Resistant Starch[J].Journal of Agricultural and Food Chemistry, 2007, 55 (4) :1574-1581.
[3] 大隈一裕, 西端丰秀.水溶性膳食纤维Fibersol-2[J].中国食品添加剂, 2003 (5) :11-16. [4] BANGOURA A O.Fibersol-2的制备及其生理功能的研究[D].无锡:江南大学, 2005. [5] 黄冬冬, 寇秀颖, 李春荣, 等.一种抗性麦芽糊精的制备工艺:中国, CN1908017A[P].2006. [6] 滕健.微波法抗性麦芽糊精的制备及其性质和应用的研究[D].无锡:江南大学, 2009. [7] 周焕霞.抗性糊精的特性、功能及市场前景[J].发酵科技通讯, 2011, 40 (4) :54-56. [8] 莫开菊, 谢笔均, 汪兴平, 等.葛仙米多糖的提取、分离与纯化技术研究[J].食品科学, 2004, 25 (10) :103-108. [9] 王满力, 吴英华, 吴惠芳.从猕猴桃皮渣中提取果胶的工艺研究[J].食品科技, 2003 (3) :85-86. [10] 刘步明, 曹艳萍.从海红果皮渣中提取果胶的工艺研究[J].食品科学, 2005, 26 (8) :191-193. [11] 陈改荣.胡萝卜果胶最佳萃取工艺条件的研究[J].河南化工, 1996 (8) :18-20. [12] 高华, 刘坤, 于兹东, 等.硫酸软骨素生产新工艺研究[J].青岛大学学报 (工程技术版) , 2003, 18 (4) :55-58. [13] 大隈一裕, 刘凌.难消化糊精Fibersol-2的保健功效[J].中国食物与营养, 2002 (1) :50-52. [14] Wang YJ, Delgado GA, Kozlowski R.Enzyme resistant dextrins from high amylose corn mutant starches[J].STARCH-STARKE, 2001, 53 (1) :21-26.
[15] 张攀峰, 陈玲, 李琳, 等.不同直链/支链比的玉米淀粉分子质量及其构象[J].食品科学, 2010, 31 (19) :157-160.
计量
- 文章访问数: 234
- HTML全文浏览量: 20
- PDF下载量: 227