全麦粉水不溶性戊聚糖碱法提取工艺的研究
详细信息Study on the extracting process of water unextractable pentosan of wheat
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摘要: 全麦粉中水不溶性戊聚糖(water unetractable pentosan,WUP)含量较普通面粉高,因此WUP与面筋蛋白之间的相互作用对面团的流变性质及全面面包等产品有较大的影响。本研究以全麦粉为原料,研究了其中水不溶性戊聚糖的碱法提取工艺,应用响应面分析法进行了工艺优化,最佳提取工艺条件为:料水比1∶188(g/mL),温度65℃,提取时间3h,提取率达31.87%。在最佳工艺条件下得到的提取物总糖,戊聚糖及糖醛酸含量分别为95.33%,92.09%及3.24%。Abstract: There was more water infusibility pentosan in whole meal flour than in ordinary. WUP and protein had stronger interaction with each other, and the ineraction affected dough rheological properties and bread. The extracting process of wholemeal flour water infusibility pentosan by alkali method was studied. The process was optimized by response surface methodology ( RSM) and the optimum condition was determined as that when the ratio of solid to liquid, temperature and time were 1 ∶188 ( g /mL) , 65℃ and 3h respectively. The product obtained under that condition contains 95.33% of total sugar, 92.09% of pentosan and 3.24% of uronic acid.
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[1] Courtin C M, Delcour J A.Arabinoxlans and endoxylanase in wheat flour bread-making[J].Journal of Cereal Science, 2002, 35:225-243.
[2] 李利民, 侯业茂, 朱永义, 等.谷物戊聚糖国内外研究进展[J].粮油加工与食品机械, 2002 (5) :36-38. [3] Sarker D K, Wilde P J.Enhancement of protein foam stability by formation of wheat arabinoxylan-protein crosslinks[J].Cereal Chemistry, 1998, 75:493-499.
[4] Wang M, Hamer R J.Effect of water unextractable solids on gluten formation and properties:mechanistic considerations[J].Journal of Cereal Science, 2003, 37:55-64.
[4] Bergmans M E F, Beldman G H, Gruppen, et al.Optimisation of the selective extraction of (Glucurono) arabinoxylans from wheat bran:use of barium and calcium hydroxide solution at elevated temperatures[J].Journal of Cereal Science, 1996, 23:235-245.
[5] Barron C, Robert P, Fabienne G, et al.Structural heterogeneity of wheat arabinoxylans revealed by Raman spectroscopy[J].Carbohydrate Research, 2006, 341:1186-1191.
[5] Wang M, Oudgenoeg G.Interaction of water unextractable solids with gluten protein:effect on dough properties and gluten quality[J].Journal of Cereal Science, 2003, 38:95-104.
[6] Gruppen H, Komelink F J M, Voragen A G J.Water-unextractable cell wall material from wheat flour.III.A structural model for arabinoxylans[J].Journal of Cereal Science, 1993, 19:111-128.
[6] Wang M, Vliet T V.Interaction of water unextractable solids and xylanase with gluten protein:effect of wheat cultivar[J].Journal of Cereal Science, 2005, 41:251-258.
[7] Izydorczyk M S, Biliaderis C G.Cereal arabinoxylans:advances in structure and physicochemical properties[J].Carbohydrate Polymers, 1995, 28:33-48.
[8] Faurot A-L, Saulnier L, Brot S, et al.Large scale isolation of water-soluble and water-insoluble pentosans from wheat flour[J].Lebensm-Wiss u-Technol, 1995, 28:436-441.
[9] 周素梅.阿拉伯木聚糖在焙烤制品中的功能性质的研究[D].无锡:无锡轻工大学食品学院, 2000. [10] Maes C, Delcour J A.Structural characterisation of water-extractable and water-unextractable arabinoxylans in wheat bran[J].Journal of Cereal Science, 2002, 35:315-326.
[11] 郑学玲.小麦麸皮戊聚糖的分离制备、理化性质及功能特性研究[D].无锡:江南大学食品学院, 2002. [12] Verbruggen M A, Beldman G, Voragen A G J.The selective extraction of glucuronoarabinoxylans from sorghum endosperm cell walls using barium and potassium hydroxide solutions[J].Journal of Cereal Science, 1995, 21:271-282.
[13] Hollmann J, Lindhauer M G.Pilot-scale isolation of glucuronoarabinoxylans from wheat bran[J].Carbohydrate Polymers, 2005, 59:225-230.
[14] 李建武.生物化学实验原理与方法[M].北京:北京大学出版社, 1997:25-29. [15] 周素梅, 王璋, 许时婴.面粉中戊聚糖含量测定方法的探讨[J].食品工业科技, 2000, 21 (6) :70-72. [16] 王璋, 许时婴.食品化学[M].北京:中国轻工业出版社, 2006:33-52. [17] Izydorczyka M S, MacGregor A W.Evidence of intermolecular interactions ofβ-glucans and arabinoxylans[J].Carbohydrate Polymers, 2000, 41:417-420.
[18] Mandalari G, Faulds C B, Sancho A I, et al.Fractionation and characterisation of arabinoxylans from brewers’spent grain and wheat bran[J].Journal of Cereal Science, 2005, 42:205-212.
[19] Huisman M M H, Schols H A, Voragen A G J.Glucuronoarabinoxylans from maize kernel cell walls are more complex than those from sorghum kernel cell walls[J].Carbohydrate Polymers, 2000, 43:269-279.
[20] Cyran M, Courtin C M, Delcour J A.Heterogeneity in the fine structure of alkali-extractable arabinoxylans isolated from two rye flours with high and low breadmaking quality and their coexistence with other cell wall components[J].Journal of Agricultulure and Food Chemistry, 2004, 52 (9) :2671-2680.
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